Salunkhe M, Pulusu VS et al (2024) Integrated approach of white analytical chemistry and analytical quality by design to multipurpose RP-HPLC method for synchronous estimation of multiple fixed-dose combinations of paracetamol. Chem Afr 7:1353–1371. https://doi.org/10.1007/s42250-023-00819-9

Article  CAS  Google Scholar 

Pulusu VS, Shah S (2024) Design of experiments and white analytical chemistry-driven green and sensitive spectrofluorimetric estimation of pregabalin in its pharmaceutical dosage forms and spiked human plasma. Fut J Pharm Sci 10:43. https://doi.org/10.1186/s43094-024-00615-3

Article  Google Scholar 

Ahmer MF, Ullah Q (2022) Development and applications of deep eutectic solvents in different chromatographic techniques. JPC-J Planar Chromat 35:549–570. https://doi.org/10.1007/s00764-022-00216-x

Article  CAS  Google Scholar 

Ullah Q, Khan SA, Mohammad A (2021) Applications of green solvents in thin-layer chromatography (TLC)—An overview. JPC-J Planar Chromat 34:5–29. https://doi.org/10.1007/s00764-021-00085-w

Article  CAS  Google Scholar 

Rana B, Pulusu VS et al (2024) Multipurpose RP-HPLC method for simultaneous estimation of fixed-dose combinations of anti-diabetic drugs: integrating green, economical, and robust approaches with design of experiments and white analytical chemistry. Chemi Afr 7:1385–1400. https://doi.org/10.1007/s42250-023-00835-9

Article  CAS  Google Scholar 

Sathuluri K, Bakam R, Jain R et al (2024) Analytical quality by design (AQbD) in the ICHQ14 guidelines for analytical procedure development. Accred Qual Assur 30:1–14. https://doi.org/10.1007/s00769-024-01587-w

Article  Google Scholar 

Reid GL, Morgado J, Barnett K, Harrington B, Wang J, Harwood J, Fortin D (2013) Analytical quality by design (AQbD) in pharmaceutical development. Am Pharm Rev 144191

Rana B, Pulusu VS, Shah S (2023) Simultaneous chromatographic estimation of vildagliptin and dapagliflozin using hybrid principles of white analytical chemistry and analytical quality by design. J AOAC Int 108:1–15

Google Scholar 

Shahi A, Acharya A, Pulusu VS, Shah S (2023) Implementation of white analytical chemistry–assisted analytical quality by design approach to green liquid chromatographic method for concomitant analysis of anti-hypertensive drugs in human plasma. J Chromatogr Sci 054:1–15

Google Scholar 

Pulusu VS, Shah S (2023) Principles of white analytical chemistry and design of experiments to stability-indicating chromatographic method for simultaneous estimation of thiocolchicoside and lornoxicam. J AOAC Int 106(06):1654–1665

PubMed  Google Scholar 

Drug data bank of baclofen:https://go.drugbank.com/drugs/DB00181Accessed on 14 October 2023.

Hosseinimehr SJ, Pourmorad F, Moshtaghi E, Amini M (2010) Colorimetric determination of baclofen with ninhydrin reagent and compare with HPLC method in tablet. Asian J Chem 22(1):522

CAS  Google Scholar 

Fadhil G (2017) Flow injection spectrophotometric determination of baclofen in pharmaceutical formulation using Prussian blue reaction. Al-Nahrain J Sci 20(1):17–24

Google Scholar 

El-Yazbi AF, Guirguis KM, Bedair MM, Belal TS (2019) Simple mix-and-read assays for the determination of baclofen in pharmaceutical formulation. Heliyon 5(6):e01854

PubMed  PubMed Central  Google Scholar 

Ersoy L (1985) A spectrophotometric method for the determination of baclofen. Pharmazie 40(11):803–804

CAS  PubMed  Google Scholar 

Dukova OA, Krasnov EA, Efremov AA (2015) Development of an HPLC method for determining baclofen. Pharm Chem J48:687–689

Google Scholar 

Sowjanya G, Sankar DG, Rao JS (2017) RP-HPLC method development and validation for the determination of baclofen in injections. World J Pharm Res 6(12):821–835

CAS  Google Scholar 

Sallerin-caute B, Monsarrat B, Lazorthes Y, Cros J, Bastide R (1988) A sensitive method for the determination of baclofen in human CSF by high performance liquid chromatography. J Liq Chromatogr 11(8):1753–1761

CAS  Google Scholar 

Adhao VS, Thenge RR (2017) Development and validation of stability indicating high performance liquid chromatography method for determination of baclofen. Am J Pharmtech Res 7:544–556

CAS  Google Scholar 

Millerioux L, Brault M, Gualano V, Mignot A (1996) High-performance liquid chromatographic determination of baclofen in human plasma. J Chromatogr A 729(1–2):309–314

CAS  PubMed  Google Scholar 

Saleh SF, Omar MA, Derayea SM (2016) Validated stability-indicating HPTLC determination of baclofen in bulk drug, pharmaceutical formulations and real human urine and plasma. J Adv Chem 8(1):1546–1556

Google Scholar 

Abu-Hassan AA, Ali R, Derayea SM (2021) A new convenient methodology based on dihydropyridine derivative for selective fluorimetric analysis of baclofen: application to spiked urine and content uniformity evaluation. Spectrochim Acta A: Mol Biomol Spectrosc 248:119165

CAS  PubMed  Google Scholar 

Saleh HM, El-Henawee MM, Ragab GH, Abd El-Hay SS (2007) Utility of NBD-Cl for the spectrophotometric determination of some skeletal muscle relaxant and antihistaminic drugs. Spectrochim Acta A Mol Biomol Spectrosc 67(5):1284–1289

PubMed  Google Scholar 

Ersoy L (1985) Fluorimetric determination of baclofen [γ-amino-β-(p-chlorophenyl) butyric acid]. Analyst 110(7):881–882

CAS  PubMed  Google Scholar 

Ersoy L (1990) Fluorodensitometric determination of baclofen. Analyst 115(12):1559–1560

CAS  PubMed  Google Scholar 

Tosunoǧlu S, Ersoy L (1995) Determination of baclofen in human plasma and urine by high-performance liquid chromatography with fluorescence detection. Analyst 120(2):373–375

PubMed  Google Scholar